HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanolamine → HCID 152428, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanolamine | HCID 700 | — |
| Reactant | 2-Methoxybenzaldehyde | HCID 8658 | — |
| Reactant | Hydantoin | HCID 10006 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 152428 | HCID 152428 | 90.5% |
Reaction Steps
A mixture of o-methoxybenzaldehyde (2.00 g., 14.7 moles) and hydantoin (1.47 g., 1 molar ratio) in water (12ml) was heated to 70°; monoethanolamine (1.35 g., 1.5 molar ratio) was then added. The mixture was heated in an oil bath (90°-92° ) and stirred magnetically for 4 hours. Usual workup gave the title compound as an orange solid (2.90 g.), m.p. 174°-179°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04065571 |
| Source dataset | uspto-grants-1977_12 |
| ORD ID | ord-06ee06d1617c47dfa039b7b272c245db |
| Source note | uspto-grants-1977_12 |