HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Iodide → HCID 13021430, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Iodide | HCID 5238 | — |
| Reactant | HCID 13021429 | HCID 13021429 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 13021430 | HCID 13021430 | 91.1% |
Reaction Steps
3-(Diacetoxymethyl)-4-acetoxybenzyl chloride (987 g., 3.14 mole) and sodium iodide (494 g., 3.29 moles) in 3.5 liters acetone are refluxed for 6 hours. The reaction mixture is filtered, the filtrate is evaporated to dryness, triturated in ether and filtered to yield 1,162 g (91%) of 3-(diacetoxymethyl)-4-acetoxybenzyl iodide, m.p. 117°-120° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04065572 |
| Source dataset | uspto-grants-1977_12 |
| ORD ID | ord-78cdcb0e8b2e413ab66eff35ebff3dce |
| Source note | uspto-grants-1977_12 |