HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 12595613, compound → HCID 12595637, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 12595613 | HCID 12595613 | — |
| Reactant | 4-(4-Chlorophenyl)-4-(dimethylamino)cyclohexan-1-one | HCID 12595650 | — |
| Product | HCID 12595637 | HCID 12595637 | 64% |
Reaction Steps
Following the procedure of Example 2, but substituting the appropriate quantity of 4-dimethylamino-4-(2-thienyl)cyclohexanone ethylene ketal (prepared above in Example 27H) for the 4-(p-chlorophenyl)-4-dimethylaminocyclohexanone, ethylene ketal hydrochloride there is prepared (after recrystallization from methanol-water) the title compound in 64% yield, m.p. 102°-103° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04065573 |
| Source dataset | uspto-grants-1977_12 |
| ORD ID | ord-c982d637273c4aab89fdd32d25ba4e05 |
| Source note | uspto-grants-1977_12 |