1-[1,5-Di-(2-norbornyl)-3-pentyl]-5-(2,3-dihydroxypropyl)-9,9-di-(2,3-dihydroxypropyl)-1,5,9-triazanonane → 1-[1,5-Di-(2-norbornyl)-3-pentyl]-5-(2,3-dihydroxypropyl)-1,5,9-triazanonane

HRID 462326Notes

Reaction equation

HRID 462326 reaction equation
OC(CO)CN(CC(O)CO)CCCN.OC(CO)CN(CC(O)CO)CCCN(CC(O)CO)CCCN.[CH:40]12[CH2:46][CH:43]([CH2:44][CH2:45]1)[CH2:42][CH:41]2[CH2:47][CH2:48][CH:49]([NH:59][CH2:60][CH2:61][CH2:62][N:63]([CH2:78][CH:79]([OH:82])[CH2:80][OH:81])[CH2:64][CH2:65][CH2:66][N:67](CC(O)CO)CC(O)CO)[CH2:50][CH2:51][CH:52]1[CH2:57][CH:56]2[CH2:58][CH:53]1[CH2:54][CH2:55]2>>[CH:40]12[CH2:46][CH:43]([CH2:44][CH2:45]1)[CH2:42][CH:41]2[CH2:47][CH2:48][CH:49]([NH:59][CH2:60][CH2:61][CH2:62][N:63]([CH2:78][CH:79]([OH:82])[CH2:80][OH:81])[CH2:64][CH2:65][CH2:66][NH2:67])[CH2:50][CH2:51][CH:52]1[CH2:57][CH:56]2[CH2:58][CH:53]1[CH2:54][CH2:55]2

Participants

4

Reactant 3

HCID 213906231-[1,5-Di-(2-norbornyl)-3-pentyl]-5-(2,3-dihydroxypropyl)-9,9-di-(2,3-dihydroxypropyl)-1,5,9-triazanonaneHCID 234677983,3'-[(3-Aminopropyl)azanediyl]di(propane-1,2-diol)HCID 234678171,1,5-Tri-(2,3-dihydroxypropyl)-1,5,9-triazanonane

Product 1

HCID 213906271-[1,5-Di-(2-norbornyl)-3-pentyl]-5-(2,3-dihydroxypropyl)-1,5,9-triazanonane

Procedure

In a like manner and using analogous quantities, but employing N,N-di-(2,3-dihydroxypropyl)trimethylenediamine and 1,1,5-tri-(2,3-dihydroxypropyl)-1,5,9-triazanonane instead of 3,3'-(2,3-dihydroxypropylimino)bispropylamine there are prepared respectively N-[1,5-di-(2-norbornyl)-3-pentyl]-N'-di-(2,3-dihydroxypropyl)trimethylenediamine, and 1-[1,5-di-(2-norbornyl)-3-pentyl]-5-(2,3-dihydroxypropyl)-9,9-di-(2,3-dihydroxypropyl)-1,5,9-triazanonane.

Sources & evidence

ORD record
ord-6f094efbb5284ca7a52f5ee9ba0c6575
Source dataset
uspto-grants-1977_12
Patent number
US04065497

Reaction notes

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