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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 462338Generated: October 30, 2026

Sodium Methoxide → 2-Cyclopropyl-4-methoxy-6-(trichloromethyl)-1,3,5-triazine

https://huagongshe.com/reaction/462338

Reaction equation

Participants

RoleNameHCIDCharge
ReactantSodium MethoxideHCID 10942334—
Reactant2-Cyclopropyl-4,6-bis-trichloromethyl-1,3,5-triazineHCID 20199613—
SolventMethanolHCID 887—
Product2-Cyclopropyl-4-methoxy-6-(trichloromethyl)-1,3,5-triazineHCID 20199618—

Reaction Steps

To a solution of 48 g of 2-cyclopropyl-4,6-bis-(trichloromethyl)-1,3,5-triazine in 200 ml of MeOH are added, with stirring, 4.9 g of sodium methylate, and the mixture is stirred for 1 hour at room temperature; it is then filtered and the filtrate is evaporated to dryness. The yield is 28.5 g of the title compound as a light-red oil, which solidifies after some time, m.p. 49°-51° C.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04515626
Source datasetuspto-grants-1985_05
ORD IDord-123c62b60c094bd3809ef41bb9934d9e
Source noteuspto-grants-1985_05