Hydrochloric Acid → HCID 178460139, compound

Participants

Reaction Conditions

Reaction Steps

Into 10 ml of ethanol, 2.8 g of 2-propionyl-5-(2-ethylthiopropyl)-4-methylcyclohexane-1,3-dione was dissolved and 1 g of allyloxyamine was dropped thereto at 0° C. and the resulting solution was stirred at room temperature for 3 hours. After pouring the reaction solution into ice-cold water and acidifying the mixture with hydrochloric acid, the mixture was extracted with chloroform. The chloroform solution was washed with water and dried over anhydrous magnesium sulfate. The removal of chloroform by distillation under reduced pressure gave 2.9 g of the desired product as yellow oily material. Yield 86%, nD18.5 1.5389.

Provenance & Evidence