Acetone → HCID 56989492, compound

Participants

Reaction Steps

A mixture of 0.80 g of 7-chlorohepta-3,4-dien-1-ol t-butyldimethylsilyl ether, 1.0 g of sodium iodide and 5 ml of acetone were refluxed for 24 hours. The reaction mixture was cooled and diluted with 50 ml water. The product was extracted with 100 ml of ether and the ethereal solution washed with brine, dried over potassium carbonate and evaporated to give 7-iodohepta-4,5-dien-1-ol t-butyldimethylsilyl ether.

Provenance & Evidence