Potassium Hydroxide → HCID 86740086, compound

HRID 462394Notes

Reaction equation

HRID 462394 reaction equation
[C:1]([O:22]C)(=[O:21])[CH2:2][CH2:3][CH:4]=[C:5]=[CH:6][CH2:7]/[CH:8]=[CH:9]\[CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH3:20].[OH-].[K+:25]>C(O)C>[C:1]([O-:22])(=[O:21])[CH2:2][CH2:3][CH:4]=[C:5]=[CH:6][CH2:7]/[CH:8]=[CH:9]\[CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH3:20].[K+:25]

Participants

4

Reactant 2

HCID 14797Potassium HydroxideHCID 86740085HCID 86740085, compound

Product 1

HCID 86740086HCID 86740086, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

A solution of 160 mg of methyl 4,5,8Z-eicosatrienoate in 20 ml of ethanol was treated 0.5 ml of 1.0N aqueous potassium hydroxide and the reaction mixture was stirred under nitrogen at room temperature for 7 hours. The solvents were removed under reduced pressure and the resulting oil was dried for several hours at 0.02 mn and 25° C. to give 168 mg of potassium 4,5,8Z-eicosatrienoate.

Workup

  1. customThe solvents were removed under reduced pressure
  2. customthe resulting oil was dried for several hours at 0.02 mn and 25° C.

Sources & evidence

ORD record
ord-49e1f485160e4dd4905a31f74048762f
Source dataset
uspto-grants-1985_05
Patent number
US04515727

Reaction notes

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