HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 59436548, compound → 4-(4-chloro-2-(1H-pyrazol-4-yl)phenoxy)-3-cyano-N-(1,2,4-thiadiazol-5-yl)benzenesulfonamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 59436548 | HCID 59436548 | — |
| Reactant | (4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1H-pyrazole | HCID 66820218 | — |
| Product | 4-(4-chloro-2-(1H-pyrazol-4-yl)phenoxy)-3-cyano-N-(1,2,4-thiadiazol-5-yl)benzenesulfonamide | HCID 46840949 | — |
Reaction Steps
The title compound was prepared from 4-(4-chloro-2-iodophenoxy)-3-cyano-N-(1,2,4-thiadiazol-5-yl)benzenesulfonamide (Preparation 355) and (4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1H-pyrazole using Method E above with microwave irradiation for 1 hour at 85° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08541588B2 |
| Source dataset | uspto-grants-2013_09 |
| ORD ID | ord-8c07fb10c0e44c3ba6b3347caf862fb7 |
| Source note | uspto-grants-2013_09 |