Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Benzene | HCID 241 | — |
| Reactant | Cyclopentanol | HCID 7298 | — |
| Reactant | Sodium | HCID 5360545 | — |
| Reactant | HCID 13589667 | HCID 13589667 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 56622205 | HCID 56622205 | — |
Reaction Steps
24.11 g of cyclopentanol and then 1.63 g of sodium are introduced into a 250 ml round-bottomed flask. The mixture is heated at 110°-120° C. until the sodium has disappeared. The mixture is then cooled and 80 cc of benzene are added. 26.77 g of 2-(4-benzyloxyphenyl)ethanol tosylate are then introduced in portions. The mixture is heated at 80° C. for 3 hours. The benzene is driven off, the residue is taken up in water and the solution is extracted with ethyl acetate. This gives an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04515814 |
|---|
| Source dataset | uspto-grants-1985_05 |
|---|
| ORD ID | ord-52e56f875e71462a96a71b838f50f613 |
|---|
| Source note | uspto-grants-1985_05 |
|---|
