Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Iodoethane | HCID 6340 | — |
| Reactant | Benzothiazole, 6-methoxy-2,5-dimethyl- | HCID 114285 | — |
| Product | HCID 20398555 | HCID 20398555 | — |
Reaction Steps
6 g of 2,5-dimethyl-6-methoxy-benzothiazole and 60 ml of ethyl iodide were reacted in a pressure flask heated to 100° C. on an oil bath for 3 days. After cooling, the raw product was washed by grinding with ether and acetone and dried in a desicator. It was then crystallized from ethanol, thus obtaining 54 g of a crystalline product melting at 249°-252° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04515888 |
|---|
| Source dataset | uspto-grants-1985_05 |
|---|
| ORD ID | ord-47cbabf866b04c6f968a5b4a38d43f9e |
|---|
| Source note | uspto-grants-1985_05 |
|---|
