HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acrylic Acid → Benzoic Acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acrylic Acid | HCID 6581 | — |
| Reactant | Tetrahydrofuran | HCID 8028 | — |
| Reactant | Aluminium lithium hydride | HCID 21226445 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | Benzoic Acid | HCID 243 | — |
Reaction Steps
Following the procedure of Example 1, "Westvaco 1550 Diacid" was reduced by lithium aluminum hydride in tetrahydrofuran to a diol having formula VIII in which m is 5, p is 7 and the broken line indicates a double bond. This diol (85 grams, 0.25 mole) was reacted with acrylic acid (90 ml., 1.28 mole) in toluene solution to yield the desired diacylate as a liquid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04515931 |
| Source dataset | uspto-grants-1985_05 |
| ORD ID | ord-f6986dfbff1a48e5a805f2975b41f447 |
| Source note | uspto-grants-1985_05 |