HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → 1-[1-(2,2-Diethoxyethyl)cyclohexyl]methanamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Sodium | HCID 5360545 | — |
| Reactant | 1-(2,2-Diethoxyethyl)cyclohexane-1-carbonitrile | HCID 13217350 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 1-[1-(2,2-Diethoxyethyl)cyclohexyl]methanamine | HCID 13217351 | — |
Reaction Steps
90 g of di-(ethyloxy)ethyl-cyclohexane-carbonitrile are dissolved in 1 l of ethanol, and 60 g of sodium are added. After dissolution of the metal, 100 ml of water are added, and the solvent is substantially removed in vacuo. 300 ml of water are added to the residue, and it is extracted three times with 200 ml of ether. The ethereal phase is dried over sodium sulfate, concentrated, and distilled in vacuo.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04515960 |
| Source dataset | uspto-grants-1985_05 |
| ORD ID | ord-152fbe1c9360470ea310516901618837 |
| Source note | uspto-grants-1985_05 |