HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl Bromide → HCID 13051544, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl Bromide | HCID 7498 | — |
| Reactant | Sodium Carbonate | HCID 10340 | — |
| Reactant | Chromanone | HCID 68110 | — |
| Reactant | HCID 13051538 | HCID 13051538 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 13051544 | HCID 13051544 | — |
Reaction Steps
3.5 g of the crude product from Example 4 were converted to the above chromanone, using 7 g of benzyl bromide, 3 of Na2CO3 and 15 ml of dimethylformamide, by a method similar to that of Example 9. Yield (after purification three times by chromatography): 20%; melting point: 51°-62° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04515975 |
| Source dataset | uspto-grants-1985_05 |
| ORD ID | ord-0d3150a461d64ff0a0f7c6d4b25f786f |
| Source note | uspto-grants-1985_05 |