Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Triisopropyl phosphite → HCID 86740094, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Triisopropyl phosphite | HCID 8304 | — |
| 반응물 | Phosphite | HCID 107908 | — |
| 반응물 | 5-(2-Chloro-4-(trifluoromethyl)phenoxy)-2-nitrobenzoyl chloride | HCID 3017765 | — |
| 용매 | Diethyl Ether | HCID 3283 | — |
| 생성물 | HCID 86740094 | HCID 86740094 | — |
반응 단계
To a stirred solution of 5-[2-chloro-4-(trifluoromethyl)phenoxy]-2-nitrobenzoyl chloride (3.8 g, 0.01 mole) in ether (100 ml) was added triisopropyl phosphite (2.1 g, 0.01 mole). The reaction was refluxed for one hour and the disappearance of phosphite monitored by v.p.c.. The ether was stripped off and the resulting oil placed under vacuum (1.0 mm) at 40° C. for two hours. The resulting amber liquid amounted to 5.2 g.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04517010 |
| 출처 데이터셋 | uspto-grants-1985_05 |
| ORD ID | ord-d663a8a07cc54c2ca4b3463d9951d83c |
| 출처 메모 | uspto-grants-1985_05 |