2,6-Dichlorobenzoic acid → HCID 11759162, compound

HRID 462683Notes

Reaction equation

HRID 462683 reaction equation
[Cl:1][C:2]1[CH:10]=[CH:9][CH:8]=[C:7]([Cl:11])[C:3]=1[C:4]([OH:6])=O.[CH3:12][O:13][C:14]1[CH:19]=[CH:18][C:17]([CH3:20])=[CH:16][C:15]=1[O:21][CH3:22]>>[Cl:11][C:7]1[CH:8]=[CH:9][CH:10]=[C:2]([Cl:1])[C:3]=1[C:4]([C:18]1[C:17]([CH3:20])=[CH:16][C:15]([O:21][CH3:22])=[C:14]([O:13][CH3:12])[CH:19]=1)=[O:6]

Participants

3

Reactant 2

HCID 57582,6-Dichlorobenzoic acidHCID 681263,4-Dimethoxytoluene

Product 1

HCID 11759162HCID 11759162, compound

Procedure

Reaction of 9.5 g (0.05 mol) of 2,6-dichlorobenzoic acid and 7.5 g (0.05 mol) of 1,2-dimethoxy-4-methylbenzene, in a manner analogous to that of Example 3(a), yields (2,6-dichlorophenyl)-(3,4-dimethoxy-6-methyl-phenyl)-methanone as colourless crystals, m.p. 101°-103° C.

Sources & evidence

ORD record
ord-62b239c3f9b1410fb28bd5f9f1f025e1
Source dataset
uspto-grants-1985_05
Patent number
US04517184

Reaction notes

Loading…