HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Anhydride → 7-Acetoxy-3-methoxybicyclo[4,3,0]non-3-ene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | 7-Hydroxy-3-methoxybicyclo[4,3,0]non-3-ene | HCID 13240998 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | 7-Acetoxy-3-methoxybicyclo[4,3,0]non-3-ene | HCID 13240999 | 91.7% |
Reaction Steps
Acetic anhydride (62.3 g) was added to a solution of 7-hydroxy-3-methoxybicyclo[4,3,0]non-3-ene (51.4 g; prepared as described in Reference Example 2) in pyridine (166 ml), and the mixture was left to stand at the ambient temperature for 60 hours. Concentration under reduced pressure gave 7-acetoxy-3-methoxybicyclo[4,3,0]non-3-ene (58.9 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04517202 |
| Source dataset | uspto-grants-1985_05 |
| ORD ID | ord-fbc8884804fb4ed18d126b4f5004d735 |
| Source note | uspto-grants-1985_05 |