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HRID46281

反应详情

EQUATION

反应方程式

HRID 46281 的结构方程式

REACTANTS

反应物

2
结构：Oc1ccc(F)cc1Br
HCID605472

2-Bromo-4-fluorophenol

C6H4BrFO

结构：N#Cc1cc(S(=O)(=O)Nc2ncns2)ccc1F
HCID58042302

未命名化合物

PRODUCTS

生成物

1
结构：N#Cc1cc(S(=O)(=O)Nc2ncns2)ccc1Oc1ccc(F)cc1Br
HCID59436571

未命名化合物

PROCEDURE

实验过程

Prepared according to the process of Preparation 51, using 2-bromo-4-fluorophenol and 3-cyano-4-fluoro-N-(1,2,4-thiadiazol-5-yl)benzenesulfonamide (Preparation 65). LCMS Rt=3.01 min MS m/z 284 [MH]+ 1HNMR (d6-DMSO): δ 6.8 (m, 1H), 7.4 (m, 1H), 7.6 (m, 1H), 7.8 (m, 1H), 8.0 (m, 1H), 8.3 (m, 1H), 8.5 (s, 1H).

WORKUP

后处理

  1. customPrepared
  2. customaccording to the process of Preparation 51