Thionyl Chloride → HCID 178444542, compound

HRID 462875Notes

Reaction equation

HRID 462875 reaction equation
[CH2:1]([C@H:6]1[CH2:11][CH2:10][C@H:9]([C:12]([OH:14])=O)[CH2:8][CH2:7]1)[CH2:2][CH2:3][CH2:4][CH3:5].S(Cl)([Cl:17])=O>>[CH2:1]([C@H:6]1[CH2:11][CH2:10][C@H:9]([C:12]([Cl:17])=[O:14])[CH2:8][CH2:7]1)[CH2:2][CH2:3][CH2:4][CH3:5]

Participants

3

Reactant 2

HCID 24386Thionyl ChlorideHCID 178444557HCID 178444557, compound

Product 1

HCID 178444542HCID 178444542, compound

Procedure

5.58 g Of trans-4-pentylcyclohexylcarboxylic acid was heated with 20 ml of thionyl chloride under reflux conditions. After the reaction was completed, the excess of thionyl chloride was removed completely under reduced pressure and the product residue obtained was distilled under reduced pressure. Trans-4-pentylcyclohexylcarbonyl chloride having a boiling point of 103° to 105° C./0.5 mmHg was obtained.

Workup

  1. customthe excess of thionyl chloride was removed completely under reduced pressure
  2. customthe product residue obtained
  3. distillationwas distilled under reduced pressure

Sources & evidence

ORD record
ord-a6066b6dbaaa4fe79ddd37f85dbd565e
Source dataset
uspto-grants-1985_05
Patent number
US04518226

Reaction notes

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