HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(4-Chlorophenyl)pent-4-en-1-ol → HCID 20281483, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(4-Chlorophenyl)pent-4-en-1-ol | HCID 13235818 | — |
| Reactant | HCID 20281480 | HCID 20281480 | — |
| Reactant | Aluminium lithium hydride | HCID 21226445 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 20281483 | HCID 20281483 | 105% |
Reaction Steps
By the procedure described for the preparation of 4-(4-chlorophenyl)pent-4-en-1-ol (see Example 1), methyl 3-ethyl-4-(4-chlorophenyl)pent-4-enoate (1.50 g) and lithium aluminium hydride (0.57 g) in dry diethyl ether (50 ml) gave 3-ethyl-4-(4-chlorophenyl)pent-4-en-1-ol (1.40 g, quantitative) as a pale yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04518415 |
| Source dataset | uspto-grants-1985_05 |
| ORD ID | ord-f85e45b30a214eccbbe3f392fc527bf4 |
| Source note | uspto-grants-1985_05 |