HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(4-Chlorophenyl)pent-4-en-1-ol → HCID 20281497, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(4-Chlorophenyl)pent-4-en-1-ol | HCID 13235818 | — |
| Reactant | HCID 20281498 | HCID 20281498 | — |
| Reactant | Aluminium lithium hydride | HCID 21226445 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 20281497 | HCID 20281497 | 91% |
Reaction Steps
By the procedure described for the preparation of 4-(4-chlorophenyl)pent-4-en-1-ol (see Example 1), 4-formyl-2-(2,4-dichlorophenyl)hept-1-ene (1.7 g) and lithium aluminium hydride (0.5 g) in dry diethyl ether (30 ml) gave 4-(hydroxymethyl)-2-(2,4-dichlorophenyl)hept-1-ene (1.55 g, 91%) as a colourless oil, 1H nmr (CDCl3): δ3.52 (2H, d J 6 Hz, CH2OH).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04518415 |
| Source dataset | uspto-grants-1985_05 |
| ORD ID | ord-abd91127b23c45c0ab0b45b2cb0a9bcd |
| Source note | uspto-grants-1985_05 |