HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Cyclohexylbenzene-1-thiol → 6-[4-(4-Cyclohexyl-phenylmercapto)-butoxy]-4,4-di-n-hexyl-4H-3,1-benzoxazin-2-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Cyclohexylbenzene-1-thiol | HCID 12455966 | — |
| Reactant | 6-(4-Chlorobutoxy)-4,4-dihexyl-1,4-dihydro-2H-3,1-benzoxazin-2-one | HCID 13260507 | — |
| Product | 6-[4-(4-Cyclohexyl-phenylmercapto)-butoxy]-4,4-di-n-hexyl-4H-3,1-benzoxazin-2-one | HCID 13260517 | — |
Reaction Steps
Prepared analogously to Example 1 from 6-(4-chlorobutoxy)-4,4-di-n-hexyl-4H-3,1-benzoxazin-2-one [oil, RF value: 0.7; silica gel plate; chloroform/acetone (19:1)] and 4-cyclohexyl-thiophenol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04518597 |
| Source dataset | uspto-grants-1985_05 |
| ORD ID | ord-b578cffd84f74e8a810405b2f1018631 |
| Source note | uspto-grants-1985_05 |