3,4-Dichlorobenzenethiol → 6-[4-(3,4-Dichloro-phenylmercapto)-butoxy]-4,4-dicyclohexyl-4H-3,1-benzoxazin-2-one

HRID 463091Notes

Reaction equation

HRID 463091 reaction equation
Cl[CH2:2][CH2:3][CH2:4][CH2:5][O:6][C:7]1[CH:8]=[CH:9][C:10]2[NH:15][C:14](=[O:16])[O:13][C:12]([CH:23]3[CH2:28][CH2:27][CH2:26][CH2:25][CH2:24]3)([CH:17]3[CH2:22][CH2:21][CH2:20][CH2:19][CH2:18]3)[C:11]=2[CH:29]=1.[Cl:30][C:31]1[CH:32]=[C:33]([SH:38])[CH:34]=[CH:35][C:36]=1[Cl:37]>>[Cl:30][C:31]1[CH:32]=[C:33]([S:38][CH2:2][CH2:3][CH2:4][CH2:5][O:6][C:7]2[CH:8]=[CH:9][C:10]3[NH:15][C:14](=[O:16])[O:13][C:12]([CH:23]4[CH2:28][CH2:27][CH2:26][CH2:25][CH2:24]4)([CH:17]4[CH2:22][CH2:21][CH2:20][CH2:19][CH2:18]4)[C:11]=3[CH:29]=2)[CH:34]=[CH:35][C:36]=1[Cl:37]

Participants

3

Reactant 2

HCID 799643,4-DichlorobenzenethiolHCID 132604996-(4-chlorobutoxy)-4,4-dicyclohexyl-4H-3,1-benzoxazin-2-one

Product 1

HCID 132605216-[4-(3,4-Dichloro-phenylmercapto)-butoxy]-4,4-dicyclohexyl-4H-3,1-benzoxazin-2-one

Procedure

Prepared analogously to Example 1 from 6-(4-chlorobutoxy)-4,4-dicyclohexyl-4H-3,1-benzoxazin-2-one and 3,4-dichloro-thiophenol.

Sources & evidence

ORD record
ord-79f9f8d3f4e6434c89e0e099ad46be1b
Source dataset
uspto-grants-1985_05
Patent number
US04518597

Reaction notes

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