Methanethiol → 6-(4-Methylmercapto-butoxy)-4,4-dimethyl-4H-3,1-benzoxazin-2-one

HRID 463100Notes

Reaction equation

HRID 463100 reaction equation
Cl[CH2:2][CH2:3][CH2:4][CH2:5][O:6][C:7]1[CH:8]=[CH:9][C:10]2[NH:15][C:14](=[O:16])[O:13][C:12]([CH3:18])([CH3:17])[C:11]=2[CH:19]=1.[CH3:20][SH:21]>>[CH3:20][S:21][CH2:2][CH2:3][CH2:4][CH2:5][O:6][C:7]1[CH:8]=[CH:9][C:10]2[NH:15][C:14](=[O:16])[O:13][C:12]([CH3:18])([CH3:17])[C:11]=2[CH:19]=1

Participants

3

Reactant 2

HCID 878MethanethiolHCID 132605036-(4-Chlorobutoxy)-4,4-dimethyl-1,4-dihydro-2H-3,1-benzoxazin-2-one

Product 1

HCID 132605326-(4-Methylmercapto-butoxy)-4,4-dimethyl-4H-3,1-benzoxazin-2-one

Procedure

Prepared analogously to Example 1 from 6-(4-chlorobutoxy)-4,4-dimethyl-4H-3,1-benzoxazin-2-one and methylmercaptan.

Sources & evidence

ORD record
ord-f5f9ffaa05e54bc0a20e7543988ec3de
Source dataset
uspto-grants-1985_05
Patent number
US04518597

Reaction notes

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