4-Methylbenzenethiol → 6-[4-(4-Methyl-phenylmercapto)-butoxy]-4H-3,1-benzoxazin-2-one

HRID 463102Notes

Reaction equation

Cl[CH2:2][CH2:3][CH2:4][CH2:5][O:6][C:7]1[CH:8]=[CH:9][C:10]2[NH:15][C:14](=[O:16])[O:13][CH2:12][C:11]=2[CH:17]=1.[CH3:18][C:19]1[CH:24]=[CH:23][C:22]([SH:25])=[CH:21][CH:20]=1>>[CH3:18][C:19]1[CH:24]=[CH:23][C:22]([S:25][CH2:2][CH2:3][CH2:4][CH2:5][O:6][C:7]2[CH:8]=[CH:9][C:10]3[NH:15][C:14](=[O:16])[O:13][CH2:12][C:11]=3[CH:17]=2)=[CH:21][CH:20]=1

Participants

Reactant 2

HCID 78114-Methylbenzenethiol

HCID 132605016-(4-Chlorobutoxy)-1,4-dihydro-2H-3,1-benzoxazin-2-one

Product 1

HCID 132605346-[4-(4-Methyl-phenylmercapto)-butoxy]-4H-3,1-benzoxazin-2-one

Procedure

Prepared analogously to Example 1 from 6-(4-chlorobutoxy)-4H-3,1-benzoxazin-2-one and 4-methyl-thiophenol.

Sources & evidence

ORD record: ord-e18022012e4d470b96209f80fac19816
Source dataset: uspto-grants-1985_05
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04518597

Reaction notes

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