4-Cyclohexylbenzene-1-thiol → 6-[4-(4-Cyclohexyl-phenylmercapto)-butoxy]-4H-3,1-benzoxazin-2-one

HRID 463104Notes

Reaction equation

HRID 463104 reaction equation
Cl[CH2:2][CH2:3][CH2:4][CH2:5][O:6][C:7]1[CH:8]=[CH:9][C:10]2[NH:15][C:14](=[O:16])[O:13][CH2:12][C:11]=2[CH:17]=1.[CH:18]1([C:24]2[CH:29]=[CH:28][C:27]([SH:30])=[CH:26][CH:25]=2)[CH2:23][CH2:22][CH2:21][CH2:20][CH2:19]1>>[CH:18]1([C:24]2[CH:25]=[CH:26][C:27]([S:30][CH2:2][CH2:3][CH2:4][CH2:5][O:6][C:7]3[CH:8]=[CH:9][C:10]4[NH:15][C:14](=[O:16])[O:13][CH2:12][C:11]=4[CH:17]=3)=[CH:28][CH:29]=2)[CH2:19][CH2:20][CH2:21][CH2:22][CH2:23]1

Participants

3

Reactant 2

HCID 124559664-Cyclohexylbenzene-1-thiolHCID 132605016-(4-Chlorobutoxy)-1,4-dihydro-2H-3,1-benzoxazin-2-one

Product 1

HCID 132605366-[4-(4-Cyclohexyl-phenylmercapto)-butoxy]-4H-3,1-benzoxazin-2-one

Procedure

Prepared analogously to Example 1 from 6-(4-chlorobutoxy)-4H-3,1-benzoxazin-2-one and 4-cyclohexyl-thiophenol.

Sources & evidence

ORD record
ord-959d02ab982c4ebfb30b7356875c97cf
Source dataset
uspto-grants-1985_05
Patent number
US04518597

Reaction notes

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