4'-Mercaptoacetanilide → 6-[4-(4-Acetamido-phenylmercapto)-butoxy]-4H-3,1-benzoxazin-2-one

HRID 463106Notes

Reaction equation

Cl[CH2:2][CH2:3][CH2:4][CH2:5][O:6][C:7]1[CH:8]=[CH:9][C:10]2[NH:15][C:14](=[O:16])[O:13][CH2:12][C:11]=2[CH:17]=1.[C:18]([NH:21][C:22]1[CH:27]=[CH:26][C:25]([SH:28])=[CH:24][CH:23]=1)(=[O:20])[CH3:19]>>[C:18]([NH:21][C:22]1[CH:27]=[CH:26][C:25]([S:28][CH2:2][CH2:3][CH2:4][CH2:5][O:6][C:7]2[CH:8]=[CH:9][C:10]3[NH:15][C:14](=[O:16])[O:13][CH2:12][C:11]=3[CH:17]=2)=[CH:24][CH:23]=1)(=[O:20])[CH3:19]

Participants

Reactant 2

HCID 707774'-Mercaptoacetanilide

HCID 132605016-(4-Chlorobutoxy)-1,4-dihydro-2H-3,1-benzoxazin-2-one

Product 1

HCID 132605386-[4-(4-Acetamido-phenylmercapto)-butoxy]-4H-3,1-benzoxazin-2-one

Procedure

Prepared analogously to Example 1 from 6-(4-chlorobutoxy)-4H-3,1-benzoxazin-2-one and 4-acetamido-thiophenol.

Sources & evidence

ORD record: ord-d791768fab5c45559d74c9451acb9e2a
Source dataset: uspto-grants-1985_05
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04518597

Reaction notes

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