3,4-Dichlorobenzenethiol → 6-[3-(3,4-Dichloro-phenylmercapto)-propoxy]-4,4-dimethyl-4H-3,1-benzoxazin-2-one

HRID 463108Notes

Reaction equation

HRID 463108 reaction equation
Cl[CH2:2][CH2:3][CH2:4][O:5][C:6]1[CH:7]=[CH:8][C:9]2[NH:14][C:13](=[O:15])[O:12][C:11]([CH3:17])([CH3:16])[C:10]=2[CH:18]=1.[Cl:19][C:20]1[CH:21]=[C:22]([SH:27])[CH:23]=[CH:24][C:25]=1[Cl:26]>>[Cl:19][C:20]1[CH:21]=[C:22]([S:27][CH2:2][CH2:3][CH2:4][O:5][C:6]2[CH:7]=[CH:8][C:9]3[NH:14][C:13](=[O:15])[O:12][C:11]([CH3:17])([CH3:16])[C:10]=3[CH:18]=2)[CH:23]=[CH:24][C:25]=1[Cl:26]

Participants

3

Reactant 2

HCID 799643,4-DichlorobenzenethiolHCID 132604916-(3-chloropropoxy)-4,4-dimethyl-4H-3,1-benzoxazin-2-one

Product 1

HCID 132605406-[3-(3,4-Dichloro-phenylmercapto)-propoxy]-4,4-dimethyl-4H-3,1-benzoxazin-2-one

Procedure

Prepared analogously to Example 1 from 6-(3-chloropropoxy)-4,4-dimethyl-4H-3,1-benzoxazin-2-one and 3,4-dichloro-thiophenol.

Sources & evidence

ORD record
ord-b95ee1eecaac4b9fafbf05a0ceea8b1b
Source dataset
uspto-grants-1985_05
Patent number
US04518597

Reaction notes

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