4-Cyclohexylbenzene-1-thiol → 6-[3-(4-Cyclohexyl-phenylmercapto)-propoxy]-4,4-dimethyl-4H-3,1-benzoxazin-2-one

HRID 463109Notes

Reaction equation

HRID 463109 reaction equation
Cl[CH2:2][CH2:3][CH2:4][O:5][C:6]1[CH:7]=[CH:8][C:9]2[NH:14][C:13](=[O:15])[O:12][C:11]([CH3:17])([CH3:16])[C:10]=2[CH:18]=1.[CH:19]1([C:25]2[CH:30]=[CH:29][C:28]([SH:31])=[CH:27][CH:26]=2)[CH2:24][CH2:23][CH2:22][CH2:21][CH2:20]1>>[CH:19]1([C:25]2[CH:26]=[CH:27][C:28]([S:31][CH2:2][CH2:3][CH2:4][O:5][C:6]3[CH:7]=[CH:8][C:9]4[NH:14][C:13](=[O:15])[O:12][C:11]([CH3:17])([CH3:16])[C:10]=4[CH:18]=3)=[CH:29][CH:30]=2)[CH2:20][CH2:21][CH2:22][CH2:23][CH2:24]1

Participants

3

Reactant 2

HCID 124559664-Cyclohexylbenzene-1-thiolHCID 132604916-(3-chloropropoxy)-4,4-dimethyl-4H-3,1-benzoxazin-2-one

Product 1

HCID 132605416-[3-(4-Cyclohexyl-phenylmercapto)-propoxy]-4,4-dimethyl-4H-3,1-benzoxazin-2-one

Procedure

Prepared analogously to Example 1 from 6-(3-chloropropoxy)-4,4-dimethyl-4H-3,1-benzoxazin-2-one and 4-cyclohexyl-thiophenol.

Sources & evidence

ORD record
ord-273ba92568044cf1acad1aa0a89616dc
Source dataset
uspto-grants-1985_05
Patent number
US04518597

Reaction notes

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