3,4-Xylenethiol → 6-[4-(3,4-Dimethyl-phenylmercapto)-butoxy]-4H-3,1-benzoxazin-2-one

HRID 463110Notes

Reaction equation

HRID 463110 reaction equation
Cl[CH2:2][CH2:3][CH2:4][CH2:5][O:6][C:7]1[CH:8]=[CH:9][C:10]2[NH:15][C:14](=[O:16])[O:13][CH2:12][C:11]=2[CH:17]=1.[CH3:18][C:19]1[CH:20]=[C:21]([SH:26])[CH:22]=[CH:23][C:24]=1[CH3:25]>>[CH3:18][C:19]1[CH:20]=[C:21]([S:26][CH2:2][CH2:3][CH2:4][CH2:5][O:6][C:7]2[CH:8]=[CH:9][C:10]3[NH:15][C:14](=[O:16])[O:13][CH2:12][C:11]=3[CH:17]=2)[CH:22]=[CH:23][C:24]=1[CH3:25]

Participants

3

Reactant 2

HCID 877993,4-XylenethiolHCID 132605016-(4-Chlorobutoxy)-1,4-dihydro-2H-3,1-benzoxazin-2-one

Product 1

HCID 132605426-[4-(3,4-Dimethyl-phenylmercapto)-butoxy]-4H-3,1-benzoxazin-2-one

Procedure

Prepared analogously to Example 1 from 6-(4-chlorobutoxy)-4H-3,1-benzoxazin-2-one and 3,4-dimethyl-thiophenol.

Sources & evidence

ORD record
ord-9635738adec64195a589dee9108203fb
Source dataset
uspto-grants-1985_05
Patent number
US04518597

Reaction notes

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