4-Cyclohexylbenzene-1-thiol → 6-[5-(4-Cyclohexyl-phenylmercapto)-pentoxy]-4,4-dimethyl-4H-3,1-benzoxazin-2-one

HRID 463111Notes

Reaction equation

HRID 463111 reaction equation
Br[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][O:7][C:8]1[CH:9]=[CH:10][C:11]2[NH:16][C:15](=[O:17])[O:14][C:13]([CH3:19])([CH3:18])[C:12]=2[CH:20]=1.[CH:21]1([C:27]2[CH:32]=[CH:31][C:30]([SH:33])=[CH:29][CH:28]=2)[CH2:26][CH2:25][CH2:24][CH2:23][CH2:22]1>>[CH:21]1([C:27]2[CH:28]=[CH:29][C:30]([S:33][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][O:7][C:8]3[CH:9]=[CH:10][C:11]4[NH:16][C:15](=[O:17])[O:14][C:13]([CH3:19])([CH3:18])[C:12]=4[CH:20]=3)=[CH:31][CH:32]=2)[CH2:22][CH2:23][CH2:24][CH2:25][CH2:26]1

Participants

3

Reactant 2

HCID 124559664-Cyclohexylbenzene-1-thiolHCID 132604896-(5-bromopentoxy)-4,4-dimethyl-4H-3,1-benzoxazin-2-one

Product 1

HCID 132605436-[5-(4-Cyclohexyl-phenylmercapto)-pentoxy]-4,4-dimethyl-4H-3,1-benzoxazin-2-one

Procedure

Prepared analogously to Example 1 from 6-(5-bromopentoxy)-4,4-dimethyl-4H-3,1-benzoxazin-2-one and 4-cyclohexyl-thiophenol.

Sources & evidence

ORD record
ord-e0f050eb1b054a32abcf211500c05618
Source dataset
uspto-grants-1985_05
Patent number
US04518597

Reaction notes

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