6-hydroxy-4,4-dimethyl-1,4-dihydro-2H-3,1-benzoxazin-2-one → 6-[4-(4-chlorophenylmercapto)-butoxy]-4,4-dimethyl-4H-3,1-benzoxazin-2-one

HRID 463151Notes

Reaction equation

HRID 463151 reaction equation
[OH:1][C:2]1[CH:3]=[CH:4][C:5]2[NH:10][C:9](=[O:11])[O:8][C:7]([CH3:13])([CH3:12])[C:6]=2[CH:14]=1.[Cl:15][C:16]1[CH:21]=[CH:20][C:19]([S:22][CH2:23][CH2:24][CH2:25][CH2:26]Cl)=[CH:18][CH:17]=1>>[Cl:15][C:16]1[CH:17]=[CH:18][C:19]([S:22][CH2:23][CH2:24][CH2:25][CH2:26][O:1][C:2]2[CH:3]=[CH:4][C:5]3[NH:10][C:9](=[O:11])[O:8][C:7]([CH3:12])([CH3:13])[C:6]=3[CH:14]=2)=[CH:20][CH:21]=1

Participants

3

Reactant 2

HCID 132604826-hydroxy-4,4-dimethyl-1,4-dihydro-2H-3,1-benzoxazin-2-oneHCID 540931394-(4-Chlorophenylmercapto)-butylchloride

Product 1

HCID 132605516-[4-(4-chlorophenylmercapto)-butoxy]-4,4-dimethyl-4H-3,1-benzoxazin-2-one

Procedure

Prepared analogously to Example 5 from 6-hydroxy-4,4-dimethyl-4H-3,1-benzoxazin-2-one and 4-(4-chlorophenylmercapto)-butylchloride.

Sources & evidence

ORD record
ord-6ae303334cd24e8293bd5354e7ec8e1e
Source dataset
uspto-grants-1985_05
Patent number
US04518597

Reaction notes

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