3,4-Dimethoxybenzene-1-thiol → 6-[6-(3,4-Dimethoxy-phenylmercapto)-hexyloxy]-4,4-dimethyl-4H-3,1-benzoxazin-2-one

HRID 463154Notes

Reaction equation

HRID 463154 reaction equation
Br[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][O:8][C:9]1[CH:10]=[CH:11][C:12]2[NH:17][C:16](=[O:18])[O:15][C:14]([CH3:20])([CH3:19])[C:13]=2[CH:21]=1.[CH3:22][O:23][C:24]1[CH:25]=[C:26]([SH:32])[CH:27]=[CH:28][C:29]=1[O:30][CH3:31]>>[CH3:22][O:23][C:24]1[CH:25]=[C:26]([S:32][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][O:8][C:9]2[CH:10]=[CH:11][C:12]3[NH:17][C:16](=[O:18])[O:15][C:14]([CH3:20])([CH3:19])[C:13]=3[CH:21]=2)[CH:27]=[CH:28][C:29]=1[O:30][CH3:31]

Participants

3

Reactant 2

HCID 1365393,4-Dimethoxybenzene-1-thiolHCID 13260492HCID 13260492, compound

Product 1

HCID 132605476-[6-(3,4-Dimethoxy-phenylmercapto)-hexyloxy]-4,4-dimethyl-4H-3,1-benzoxazin-2-one

Procedure

Prepared analogously to Example 1 from 6-(6-bromohexyloxy)-4,4-dimethyl-4H-3,1-benzoxazin-2-one and 3,4-dimethoxythiophenol.

Sources & evidence

ORD record
ord-11dc0b2e241b45e48293c4e042d99f88
Source dataset
uspto-grants-1985_05
Patent number
US04518597

Reaction notes

Loading…