HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-[(4-Bromobutyl)sulfanyl]-1,2-dichlorobenzene → 6-[4-(3,4-dichloro-phenylmercapto)-butoxy]-4,4-dimethyl-4H-3,1-benzoxazin-2-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-[(4-Bromobutyl)sulfanyl]-1,2-dichlorobenzene | HCID 13254021 | — |
| Reactant | 6-hydroxy-4,4-dimethyl-1,4-dihydro-2H-3,1-benzoxazin-2-one | HCID 13260482 | — |
| Product | 6-[4-(3,4-dichloro-phenylmercapto)-butoxy]-4,4-dimethyl-4H-3,1-benzoxazin-2-one | HCID 13254018 | — |
Reaction Steps
Prepared analogously to Example 4 from 6-hydroxy-4,4-dimethyl-4H-3,1-benzoxazin-2-one and 4-(3,4-dichlorophenylmercapto)-butylbromide (B.p. 0.1 mb : 153°-160° C.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04518597 |
| Source dataset | uspto-grants-1985_05 |
| ORD ID | ord-3f704899ace346d5a64b6444eb2ecf0b |
| Source note | uspto-grants-1985_05 |