3,4-Dimethoxybenzene-1-thiol → 4-Isopropyl-6-[3-(3,4-dimethoxy-phenylmercapto)-propoxy]-4H-3,1-benzoxazin-2-one

HRID 463162Notes

Reaction equation

HRID 463162 reaction equation
Cl[CH2:2][CH2:3][CH2:4][O:5][C:6]1[CH:7]=[CH:8][C:9]2[NH:14][C:13](=[O:15])[O:12][CH:11]([CH:16]([CH3:18])[CH3:17])[C:10]=2[CH:19]=1.[CH3:20][O:21][C:22]1[CH:23]=[C:24]([SH:30])[CH:25]=[CH:26][C:27]=1[O:28][CH3:29]>>[CH:16]([CH:11]1[C:10]2[CH:19]=[C:6]([O:5][CH2:4][CH2:3][CH2:2][S:30][C:24]3[CH:25]=[CH:26][C:27]([O:28][CH3:29])=[C:22]([O:21][CH3:20])[CH:23]=3)[CH:7]=[CH:8][C:9]=2[NH:14][C:13](=[O:15])[O:12]1)([CH3:18])[CH3:17]

Participants

3

Reactant 2

HCID 1365393,4-Dimethoxybenzene-1-thiolHCID 132604906-(3-chloropropoxy)-4-isopropyl-4H-3,1-benzoxazin-2-one

Product 1

HCID 132605494-Isopropyl-6-[3-(3,4-dimethoxy-phenylmercapto)-propoxy]-4H-3,1-benzoxazin-2-one

Procedure

Prepared analogously to Example 1 from 6-(3-chloropropoxy)-4-isopropyl-4H-3,1-benzoxazin-2-one and 3,4-dimethoxy-thiophenol.

Sources & evidence

ORD record
ord-022431cc2c8542309e08b20abf0f91ba
Source dataset
uspto-grants-1985_05
Patent number
US04518597

Reaction notes

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