3,4-Xylenethiol → HCID 20281860, compound

HRID 463168Notes

Reaction equation

HRID 463168 reaction equation
Cl[CH2:2][CH2:3][CH2:4][CH2:5][O:6][C:7]1[CH:8]=[CH:9][C:10]2[NH:15][C:14](=[O:16])[O:13][C:12]([CH2:19][CH3:20])([CH2:17][CH3:18])[C:11]=2[CH:21]=1.[CH3:22][C:23]1[CH:24]=[C:25]([SH:30])[CH:26]=[CH:27][C:28]=1[CH3:29]>>[CH3:22][C:23]1[CH:24]=[C:25]([S:30][CH2:2][CH2:3][CH2:4][CH2:5][O:6][C:7]2[CH:8]=[CH:9][C:10]3[NH:15][C:14](=[O:16])[O:13][C:12]([CH2:19][CH3:20])([CH2:17][CH3:18])[C:11]=3[CH:21]=2)[CH:26]=[CH:27][C:28]=1[CH3:29]

Participants

3

Reactant 2

HCID 877993,4-XylenethiolHCID 20281767HCID 20281767, compound

Product 1

HCID 20281860HCID 20281860, compound

Procedure

Prepared analogously to Example 1 from 6-(4-chlorobutoxy)-4,4-diethyl-4H-3,1-benzoxazin-2-one and 3,4-dimethyl-thiophenol.

Sources & evidence

ORD record
ord-77f7c342c7ff4a929fcda0d660b68ebd
Source dataset
uspto-grants-1985_05
Patent number
US04518597

Reaction notes

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