3,4-Xylenethiol → 8-[4-(3,4-Dimethyl-phenylmercapto)-butoxy]-4,4-dimethyl-4H-3,1-benzoxazin-2-one

HRID 463183Notes

Reaction equation

HRID 463183 reaction equation
Cl[CH2:2][CH2:3][CH2:4][CH2:5][O:6][C:7]1[C:16]2[NH:15][C:14](=[O:17])[O:13][C:12]([CH3:19])([CH3:18])[C:11]=2[CH:10]=[CH:9][CH:8]=1.[CH3:20][C:21]1[CH:22]=[C:23]([SH:28])[CH:24]=[CH:25][C:26]=1[CH3:27]>>[CH3:20][C:21]1[CH:22]=[C:23]([S:28][CH2:2][CH2:3][CH2:4][CH2:5][O:6][C:7]2[C:16]3[NH:15][C:14](=[O:17])[O:13][C:12]([CH3:19])([CH3:18])[C:11]=3[CH:10]=[CH:9][CH:8]=2)[CH:24]=[CH:25][C:26]=1[CH3:27]

Participants

3

Reactant 2

HCID 877993,4-XylenethiolHCID 202817738-(4-chlorobutoxy)-4,4-dimethyl-4H-3,1-benzoxazin-2-one

Product 1

HCID 202818208-[4-(3,4-Dimethyl-phenylmercapto)-butoxy]-4,4-dimethyl-4H-3,1-benzoxazin-2-one

Procedure

Prepared analogously to Example 1 from 8-(4-chlorobutoxy)-4,4-dimethyl-4H-3,1-benzoxazin-2-one and 3,4-dimethyl-thiophenol.

Sources & evidence

ORD record
ord-9c08e5ac1eca4d35a8cd1ed8b1beb008
Source dataset
uspto-grants-1985_05
Patent number
US04518597

Reaction notes

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