4'-Mercaptoacetanilide → HCID 20281671, compound

HRID 463186Notes

Reaction equation

CS(O[CH2:6][CH2:7][CH2:8][CH2:9][O:10][C:11]1[C:12]([N+:24]([O-:26])=[O:25])=[CH:13][C:14]2[NH:19][C:18](=[O:20])[O:17][C:16]([CH3:22])([CH3:21])[C:15]=2[CH:23]=1)(=O)=O.[C:27]([NH:30][C:31]1[CH:36]=[CH:35][C:34]([SH:37])=[CH:33][CH:32]=1)(=[O:29])[CH3:28]>>[C:27]([NH:30][C:31]1[CH:36]=[CH:35][C:34]([S:37][CH2:6][CH2:7][CH2:8][CH2:9][O:10][C:11]2[C:12]([N+:24]([O-:26])=[O:25])=[CH:13][C:14]3[NH:19][C:18](=[O:20])[O:17][C:16]([CH3:21])([CH3:22])[C:15]=3[CH:23]=2)=[CH:33][CH:32]=1)(=[O:29])[CH3:28]

Participants

Reactant 2

HCID 707774'-Mercaptoacetanilide

HCID 20281702HCID 20281702, compound

Product 1

HCID 20281671HCID 20281671, compound

Procedure

Prepared analogously to Example 210 from 6-(4-methanesulfonyloxy-butoxy)-7-nitro-4,4-dimethyl-4H-3,1-benzoxazin-2-one and 4-acetamido-thiophenol.

Sources & evidence

ORD record: ord-35bec938e34e4690b06637c064b41531
Source dataset: uspto-grants-1985_05
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04518597

Reaction notes

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