4-Methylbenzenethiol → HCID 20281782, compound

HRID 463189Notes

Reaction equation

HRID 463189 reaction equation
CS(O[CH2:6][CH2:7][CH2:8][CH2:9][O:10][C:11]1[C:12]([N+:24]([O-:26])=[O:25])=[CH:13][C:14]2[NH:19][C:18](=[O:20])[O:17][C:16]([CH3:22])([CH3:21])[C:15]=2[CH:23]=1)(=O)=O.[CH3:27][C:28]1[CH:33]=[CH:32][C:31]([SH:34])=[CH:30][CH:29]=1>>[CH3:27][C:28]1[CH:33]=[CH:32][C:31]([S:34][CH2:6][CH2:7][CH2:8][CH2:9][O:10][C:11]2[C:12]([N+:24]([O-:26])=[O:25])=[CH:13][C:14]3[NH:19][C:18](=[O:20])[O:17][C:16]([CH3:21])([CH3:22])[C:15]=3[CH:23]=2)=[CH:30][CH:29]=1

Participants

3

Reactant 2

HCID 78114-MethylbenzenethiolHCID 20281702HCID 20281702, compound

Product 1

HCID 20281782HCID 20281782, compound

Procedure

Prepared analogously to Example 210 from 6-(4-methanesulfonyloxy-butoxy)-7-nitro-4,4-dimethyl-4H-3,1-benzoxazin-2-one and 4-methyl-thiophenol.

Sources & evidence

ORD record
ord-c80516bf7563435896d097c28107b5fe
Source dataset
uspto-grants-1985_05
Patent number
US04518597

Reaction notes

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