3,4-Dimethoxybenzene-1-thiol → HCID 20281814, compound

HRID 463190Notes

Reaction equation

HRID 463190 reaction equation
CS(O[CH2:6][CH2:7][CH2:8][CH2:9][O:10][C:11]1[C:12]([N+:24]([O-:26])=[O:25])=[CH:13][C:14]2[NH:19][C:18](=[O:20])[O:17][C:16]([CH3:22])([CH3:21])[C:15]=2[CH:23]=1)(=O)=O.[CH3:27][O:28][C:29]1[CH:30]=[C:31]([SH:37])[CH:32]=[CH:33][C:34]=1[O:35][CH3:36]>>[CH3:27][O:28][C:29]1[CH:30]=[C:31]([S:37][CH2:6][CH2:7][CH2:8][CH2:9][O:10][C:11]2[C:12]([N+:24]([O-:26])=[O:25])=[CH:13][C:14]3[NH:19][C:18](=[O:20])[O:17][C:16]([CH3:21])([CH3:22])[C:15]=3[CH:23]=2)[CH:32]=[CH:33][C:34]=1[O:35][CH3:36]

Participants

3

Reactant 2

HCID 1365393,4-Dimethoxybenzene-1-thiolHCID 20281702HCID 20281702, compound

Product 1

HCID 20281814HCID 20281814, compound

Procedure

Prepared analogously to Example 210 from 6-(4-methanesulfonyloxy-butoxy)-7-nitro-4,4-dimethyl-4H-3,1-benzoxazin-2-one and 3,4-dimethoxy-thiophenol.

Sources & evidence

ORD record
ord-08d2ce3165024d72aaf8b6123567841c
Source dataset
uspto-grants-1985_05
Patent number
US04518597

Reaction notes

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