3,4-Xylenethiol → HCID 20281723, compound

HRID 463191Notes

Reaction equation

HRID 463191 reaction equation
CS(OCCCCO[C:11]1[CH:12]=[CH:13][C:14]2[NH:19][C:18](=[O:20])[O:17][C:16]([CH3:22])([CH3:21])[C:15]=2[CH:23]=1)(=O)=O.[CH3:24][C:25]1[CH:26]=[C:27]([SH:32])[CH:28]=[CH:29][C:30]=1[CH3:31]>>[CH3:24][C:25]1[CH:26]=[C:27]([S:32][CH2:13][CH2:14][CH2:15][CH2:16][O:17][C:12]2[CH:11]=[CH:23][C:15]3[C:16]([CH3:21])([CH3:22])[O:17][C:18](=[O:20])[NH:19][C:14]=3[CH:13]=2)[CH:28]=[CH:29][C:30]=1[CH3:31]

Participants

3

Reactant 2

HCID 877993,4-XylenethiolHCID 20281886HCID 20281886, compound

Product 1

HCID 20281723HCID 20281723, compound

Procedure

Prepared analogously to Example 210 from 6-(4-methanesulfonyloxy-butoxy)-4,4-dimethyl-4H-3,1-benzoxazin-2-one and 3,4-dimethyl-thiophenol.

Sources & evidence

ORD record
ord-0fffa7a2a6004122ac3cb21aef2a5043
Source dataset
uspto-grants-1985_05
Patent number
US04518597

Reaction notes

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