HCID 20281668, compound → 7-[4-(2-Pyridylmercapto)-butoxy]-4,4-dimethyl-4H-3,1-benzoxazin-2-one

HRID 463193Notes

Reaction equation

HRID 463193 reaction equation
CS(O[CH2:6][CH2:7][CH2:8][CH2:9][O:10][C:11]1[CH:23]=[CH:22][C:14]2[C:15]([CH3:21])([CH3:20])[O:16][C:17](=[O:19])[NH:18][C:13]=2[CH:12]=1)(=O)=O.[SH:24][C:25]1[CH:30]=[CH:29][CH:28]=[CH:27][N:26]=1>>[N:26]1[CH:27]=[CH:28][CH:29]=[CH:30][C:25]=1[S:24][CH2:6][CH2:7][CH2:8][CH2:9][O:10][C:11]1[CH:23]=[CH:22][C:14]2[C:15]([CH3:20])([CH3:21])[O:16][C:17](=[O:19])[NH:18][C:13]=2[CH:12]=1

Participants

3

Reactant 2

HCID 20281668HCID 20281668, compoundHCID 178418616HCID 178418616, compound

Product 1

HCID 202817217-[4-(2-Pyridylmercapto)-butoxy]-4,4-dimethyl-4H-3,1-benzoxazin-2-one

Procedure

Prepared analogously to Example 210 from 7-(4-methanesulfonyloxy-butoxy)-4,4-dimethyl-4H-3,1-benzoxazin-2-one and 2-mercapto-pyridine.

Sources & evidence

ORD record
ord-9e89be64e68542f68f6dab234b76f342
Source dataset
uspto-grants-1985_05
Patent number
US04518597

Reaction notes

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