Thiophenol → 7-(4-Phenylmercapto-butoxy)-4,4-dimethyl-4H-3,1-benzoxazin-2-one

HRID 463197Notes

Reaction equation

HRID 463197 reaction equation
CS(O[CH2:6][CH2:7][CH2:8][CH2:9][O:10][C:11]1[CH:23]=[CH:22][C:14]2[C:15]([CH3:21])([CH3:20])[O:16][C:17](=[O:19])[NH:18][C:13]=2[CH:12]=1)(=O)=O.[C:24]1([SH:30])[CH:29]=[CH:28][CH:27]=[CH:26][CH:25]=1>>[C:24]1([S:30][CH2:6][CH2:7][CH2:8][CH2:9][O:10][C:11]2[CH:23]=[CH:22][C:14]3[C:15]([CH3:20])([CH3:21])[O:16][C:17](=[O:19])[NH:18][C:13]=3[CH:12]=2)[CH:29]=[CH:28][CH:27]=[CH:26][CH:25]=1

Participants

3

Reactant 2

HCID 7969ThiophenolHCID 20281668HCID 20281668, compound

Product 1

HCID 202817127-(4-Phenylmercapto-butoxy)-4,4-dimethyl-4H-3,1-benzoxazin-2-one

Procedure

Prepared analogously to Example 210 from 7-(4-methanesulfonyloxy-butoxy)-4,4-dimethyl-4H-3,1-benzoxazin-2-one and thiophenol.

Sources & evidence

ORD record
ord-f8213f786fd740bbbc9db53e7f8c67ea
Source dataset
uspto-grants-1985_05
Patent number
US04518597

Reaction notes

Loading…