6-(4-chlorobutoxy)-4,4,8-trimethyl-4H-3,1-benzoxazin-2-one → 6-[4-(2-Pyridylmercapto)-butoxy]-4,4,8-trimethyl-4H-3,1-benzoxazin-2-one

HRID 463224Notes

Reaction equation

HRID 463224 reaction equation
Cl[CH2:2][CH2:3][CH2:4][CH2:5][O:6][C:7]1[CH:8]=[C:9]([CH3:20])[C:10]2[NH:15][C:14](=[O:16])[O:13][C:12]([CH3:18])([CH3:17])[C:11]=2[CH:19]=1.[SH:21][C:22]1[CH:27]=[CH:26][CH:25]=[CH:24][N:23]=1>>[N:23]1[CH:24]=[CH:25][CH:26]=[CH:27][C:22]=1[S:21][CH2:2][CH2:3][CH2:4][CH2:5][O:6][C:7]1[CH:8]=[C:9]([CH3:20])[C:10]2[NH:15][C:14](=[O:16])[O:13][C:12]([CH3:18])([CH3:17])[C:11]=2[CH:19]=1

Participants

3

Reactant 2

HCID 202818636-(4-chlorobutoxy)-4,4,8-trimethyl-4H-3,1-benzoxazin-2-oneHCID 178418616HCID 178418616, compound

Product 1

HCID 202818116-[4-(2-Pyridylmercapto)-butoxy]-4,4,8-trimethyl-4H-3,1-benzoxazin-2-one

Procedure

Prepared analogously to Example 1 from 6-(4-chlorobutoxy)-4,4,8-trimethyl-4H-3,1-benzoxazin-2-one and 2-mercaptopyridine.

Sources & evidence

ORD record
ord-6629b4709a824c3b94b299f44fed0755
Source dataset
uspto-grants-1985_05
Patent number
US04518597

Reaction notes

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