p-Chlorothiophenol → 6-[4-(4-Chloro-phenylmercapto)-butoxy]-4,4,8-trimethyl-4H-3,1-benzoxazin-2-one

HRID 463225Notes

Reaction equation

HRID 463225 reaction equation
Cl[CH2:2][CH2:3][CH2:4][CH2:5][O:6][C:7]1[CH:8]=[C:9]([CH3:20])[C:10]2[NH:15][C:14](=[O:16])[O:13][C:12]([CH3:18])([CH3:17])[C:11]=2[CH:19]=1.[Cl:21][C:22]1[CH:27]=[CH:26][C:25]([SH:28])=[CH:24][CH:23]=1>>[Cl:21][C:22]1[CH:27]=[CH:26][C:25]([S:28][CH2:2][CH2:3][CH2:4][CH2:5][O:6][C:7]2[CH:8]=[C:9]([CH3:20])[C:10]3[NH:15][C:14](=[O:16])[O:13][C:12]([CH3:18])([CH3:17])[C:11]=3[CH:19]=2)=[CH:24][CH:23]=1

Participants

3

Reactant 2

HCID 7815p-ChlorothiophenolHCID 202818636-(4-chlorobutoxy)-4,4,8-trimethyl-4H-3,1-benzoxazin-2-one

Product 1

HCID 202818596-[4-(4-Chloro-phenylmercapto)-butoxy]-4,4,8-trimethyl-4H-3,1-benzoxazin-2-one

Procedure

Prepared analogously to Example 1 from 6-(4-chlorobutoxy)-4,4,8-trimethyl-4H-3,1-benzoxazin-2-one and 4-chloro-thiophenol.

Sources & evidence

ORD record
ord-2580f41662c84fef86855457e3b25e2c
Source dataset
uspto-grants-1985_05
Patent number
US04518597

Reaction notes

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