Thiophenol → 6-(4-Phenylmercapto-butoxy)-4,4,8-trimethyl-4H-3,1-benzoxazin-2-one

HRID 463226Notes

Reaction equation

HRID 463226 reaction equation
Cl[CH2:2][CH2:3][CH2:4][CH2:5][O:6][C:7]1[CH:8]=[C:9]([CH3:20])[C:10]2[NH:15][C:14](=[O:16])[O:13][C:12]([CH3:18])([CH3:17])[C:11]=2[CH:19]=1.[C:21]1([SH:27])[CH:26]=[CH:25][CH:24]=[CH:23][CH:22]=1>>[C:21]1([S:27][CH2:2][CH2:3][CH2:4][CH2:5][O:6][C:7]2[CH:8]=[C:9]([CH3:20])[C:10]3[NH:15][C:14](=[O:16])[O:13][C:12]([CH3:18])([CH3:17])[C:11]=3[CH:19]=2)[CH:26]=[CH:25][CH:24]=[CH:23][CH:22]=1

Participants

3

Reactant 2

HCID 7969ThiophenolHCID 202818636-(4-chlorobutoxy)-4,4,8-trimethyl-4H-3,1-benzoxazin-2-one

Product 1

HCID 202818016-(4-Phenylmercapto-butoxy)-4,4,8-trimethyl-4H-3,1-benzoxazin-2-one

Procedure

Prepared analogously to Example 1 from 6-(4-chlorobutoxy)-4,4,8-trimethyl-4H-3,1-benzoxazin-2-one and thiophenol.

Sources & evidence

ORD record
ord-a3ace5e23eca4d31beb57f8673a81944
Source dataset
uspto-grants-1985_05
Patent number
US04518597

Reaction notes

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