8-chloro-6-hydroxy-4,4-dimethyl-4H-3,1-benzoxazin-2-one → 8-chloro-6-[4-(4-chloro-phenylmercapto)-butoxy]-4,4-dimethyl-4H-3,1-benzoxazin-2-one

HRID 463255Notes

Reaction equation

HRID 463255 reaction equation
[Cl:1][C:2]1[C:11]2[NH:10][C:9](=[O:12])[O:8][C:7]([CH3:14])([CH3:13])[C:6]=2[CH:5]=[C:4]([OH:15])[CH:3]=1.[Cl:16][C:17]1[CH:22]=[CH:21][C:20]([S:23][CH2:24][CH2:25][CH2:26][CH2:27]Cl)=[CH:19][CH:18]=1>>[Cl:1][C:2]1[C:11]2[NH:10][C:9](=[O:12])[O:8][C:7]([CH3:13])([CH3:14])[C:6]=2[CH:5]=[C:4]([O:15][CH2:27][CH2:26][CH2:25][CH2:24][S:23][C:20]2[CH:19]=[CH:18][C:17]([Cl:16])=[CH:22][CH:21]=2)[CH:3]=1

Participants

3

Reactant 2

HCID 202816978-chloro-6-hydroxy-4,4-dimethyl-4H-3,1-benzoxazin-2-oneHCID 540931394-(4-Chlorophenylmercapto)-butylchloride

Product 1

HCID 202818188-chloro-6-[4-(4-chloro-phenylmercapto)-butoxy]-4,4-dimethyl-4H-3,1-benzoxazin-2-one

Procedure

Prepared analogously to Example 4 from 8-chloro-6-hydroxy-4,4-dimethyl-4H-3,1-benzoxazin-2-one and 4-(4-chloro-phenylmercapto)-butylchloride.

Sources & evidence

ORD record
ord-e0c9ccc3a5cd4a8f83482f9086c9030a
Source dataset
uspto-grants-1985_05
Patent number
US04518597

Reaction notes

Loading…