6-hydroxy-4,4,7-trimethyl-4H-3,1-benzoxazin-2-one → 6-[4-(4-methyl-phenylmercapto)-butoxy]-4,4,7-trimethyl-4H-3,1-benzoxazin-2-one

HRID 463259Notes

Reaction equation

HRID 463259 reaction equation
[OH:1][C:2]1[C:3]([CH3:15])=[CH:4][C:5]2[NH:10][C:9](=[O:11])[O:8][C:7]([CH3:13])([CH3:12])[C:6]=2[CH:14]=1.[CH3:16][C:17]1[CH:22]=[CH:21][C:20]([S:23][CH2:24][CH2:25][CH2:26][CH2:27]Cl)=[CH:19][CH:18]=1>>[CH3:16][C:17]1[CH:22]=[CH:21][C:20]([S:23][CH2:24][CH2:25][CH2:26][CH2:27][O:1][C:2]2[C:3]([CH3:15])=[CH:4][C:5]3[NH:10][C:9](=[O:11])[O:8][C:7]([CH3:12])([CH3:13])[C:6]=3[CH:14]=2)=[CH:19][CH:18]=1

Participants

3

Reactant 2

HCID 202816846-hydroxy-4,4,7-trimethyl-4H-3,1-benzoxazin-2-oneHCID 541231844-(4-Methylphenylmercapto)-butylchloride

Product 1

HCID 202817256-[4-(4-methyl-phenylmercapto)-butoxy]-4,4,7-trimethyl-4H-3,1-benzoxazin-2-one

Procedure

Prepared analogously to Example 4 from 6-hydroxy-4,4,7-trimethyl-4H-3,1-benzoxazin-2-one and 4-(4-methyl-phenylmercapto)-butylchloride.

Sources & evidence

ORD record
ord-6f4b0046e9a147b6a79d8bebf7ec7258
Source dataset
uspto-grants-1985_05
Patent number
US04518597

Reaction notes

Loading…