5-chloro-6-hydroxy-4H-3,1-benzoxazin-2-one → 5-Chloro-6-[4-(4-methyl-phenylmercapto)-butoxy]-4H-3,1-benzoxazin-2-one

HRID 463275Notes

Reaction equation

HRID 463275 reaction equation
[Cl:1][C:2]1[C:7]2[CH2:8][O:9][C:10](=[O:12])[NH:11][C:6]=2[CH:5]=[CH:4][C:3]=1[OH:13].[CH3:14][C:15]1[CH:20]=[CH:19][C:18]([S:21][CH2:22][CH2:23][CH2:24][CH2:25]Cl)=[CH:17][CH:16]=1>>[Cl:1][C:2]1[C:7]2[CH2:8][O:9][C:10](=[O:12])[NH:11][C:6]=2[CH:5]=[CH:4][C:3]=1[O:13][CH2:25][CH2:24][CH2:23][CH2:22][S:21][C:18]1[CH:17]=[CH:16][C:15]([CH3:14])=[CH:20][CH:19]=1

Participants

3

Reactant 2

HCID 202818835-chloro-6-hydroxy-4H-3,1-benzoxazin-2-oneHCID 541231844-(4-Methylphenylmercapto)-butylchloride

Product 1

HCID 202818315-Chloro-6-[4-(4-methyl-phenylmercapto)-butoxy]-4H-3,1-benzoxazin-2-one

Procedure

Prepared analogously to Example 4 from 5-chloro-6-hydroxy-4H-3,1-benzoxazin-2-one and 4-(4-methyl-phenylmercapto)-butylchloride.

Sources & evidence

ORD record
ord-1e6facd905514d73bcd1ffe6fd3ffc2f
Source dataset
uspto-grants-1985_05
Patent number
US04518597

Reaction notes

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