HCID 20281726, compound → HCID 20281821, compound
Reaction equation
[Cl:1][C:2]1[C:7]2[C:8]([CH3:14])([CH3:13])[O:9][C:10](=[O:12])[NH:11][C:6]=2[CH:5]=[C:4]([Cl:15])[C:3]=1[OH:16].[CH3:17][C:18]1[CH:23]=[CH:22][C:21]([S:24][CH2:25][CH2:26][CH2:27][CH2:28]Cl)=[CH:20][CH:19]=1>>[Cl:1][C:2]1[C:7]2[C:8]([CH3:13])([CH3:14])[O:9][C:10](=[O:12])[NH:11][C:6]=2[CH:5]=[C:4]([Cl:15])[C:3]=1[O:16][CH2:28][CH2:27][CH2:26][CH2:25][S:24][C:21]1[CH:20]=[CH:19][C:18]([CH3:17])=[CH:23][CH:22]=1Participants
3
Procedure
Prepared analogously to Example 4 from 5,7-dichloro-6-hydroxy-4,4-dimethyl-4H-3,1-benzoxazin-2-one and 4-(4-methyl-phenylmercapto)-butylchloride.
Sources & evidence
- ORD record
- ord-2db874ab4a104c48ab9f888e369e4793
- Source dataset
- uspto-grants-1985_05
- Patent number
- US04518597
Reaction notes
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